NMR Spectroscopy
When placed in a magnetic field, all the random spins of the nuclei

align with the magnetic field
stop
reverse direction
rotate to 90° away from the induced field

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NMR Spectroscopy
Why is it important to use a deuterated solvent?

NMR uses least of this solvent
So the spectrometer can lock onto the sample to prevent the spectrum from drifting during aquisition
They dissolve polymer the fastest
Expensive solvents work best with NMR

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NMR Spectroscopy
Coupling causes the peaks in 1H NMR spectra to be split into

multiple peaks equal to the number of surrounding carbon atoms
multiple peaks equal to the number of hydrogens on surrounding atoms
multiple peaks equal to the number of hydrogen on surrounding atoms, plus one
two peaks

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NMR Spectroscopy
All hydrogen atoms

have the same resonance frequency
resonate at different frequencies depending on their environment.
are attached to carbon
resonate at about the same frequency as carbon

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